This high-pressure reactor is ideally suitable for larger experimental runs. This high-pressure reactor is available in stainless steel 1.4571 (SUS 316LTI), Hastelloy C-22, or with PTFE lining on all sides. The usable volume of the reactor can be varied between 1,000 ml and 2,240 ml using different reactor vessels.
The BR 1000/1500/2000 high-pressure reactor is notable for its ease of handling. The reactor is closed using a manual quick closure that can be attached without the use of tools. The reactor seal is established using a conical flange lock and O-ring seal of PTFE, FKM, or FFKM. The appropriate fitting inserts are available in stainless steel 1.4571 (SUS 316LTI) or Hastelloy C-22. A total of 6 connection options are provided in the lid, which can be selected from the following:
* Immersion tube for temperature probes
* Rupture disc of metal for the safe limitation of maximum pressure
* Pressure display
* Vent valve
* 2 freely selectable fittings, for example for a gas sampling valve or liquid sampling point
Temperature is regulated using a temperature probe which detects the inner temperature of the reactor in an immersion tube. A second temperature probe can optionally be used as an independent overheating safety. Appropriate stand systems are available.
Features
* 1000, 1500, 1700, 2000 or 2300 ml / 200 bar / 300℃ (PTFE-Lined 230° )
* Quick closure chain, to be operated manually without tools
* O-seal ring made of Viton®, PTFE or Kalrez®
* Either with PTFE-insert or completely made of SUS 316LTi or Hastelloy®
* Heating by elctrical or thermostated mantle
* Stiring by magnetic clutch and separate drive
* Optionally internal heating/cooling coil
* Optionally 2’nd thermocouple
Technical Specification
| BR-1000 | |||
| Material | SUS316Ti or HC | SUS316Ti PTFE | |
| Temperature max. | 300℃ | 230℃ | |
| Pressure max. | 200 bar | ||
| Reactor Vessel | Volume | approx. 1,220 ml | |
| Inner Diameter | 90 mm | ||
| Inner Height | 193 mm | ||
| Weight | approx. 10.5 kg | ||
| TFMTM-PTFE Insert* (integrated) | Volume | – | approx. 1,000 ml |
| Inner Diameter | – | 84 mm | |
| Inner Height | – | 182.5 mm | |
| Armatures | Standard Armatures | Rupture Disc, Dip Tube, Valve, Tool | |
| Pressure Measurement | analog and/or digital | ||
| Ports (total) | 6 | ||
| Ports (free) | 2** | ||
| Type of connection | 8 mm Tube Connection | ||
| Heating Systems (optional) | Electrical Heating mantle | CHM-1000 | |
| Julabo thermostat | CTM-1000 | ||
| Heating Coil | √ | ||
| Stirring | Overhead stirrer with magnetic clutch | WB20C and RV 100-SS | |
| Stand | Electric lifting stand for BR-1000 | ||
* When using PTFE inserts the maximum allowable temperature is 230℃
* The number of free ports can be enlarged by the use of T-connections
