This high-pressure reactor is attractive due to its many stirring and heating variants. It is available in stainless steel 1.4571 (SUS 316LTI), Hastelloy C-22, or with PTFE lining on all sides. The usable volume of the reactor can be varied between 310 ml and 600 ml using different reactor vessels.
The BR-300/500 high-pressure reactor is notable for its ease of handling. The reactor is closed using a manual quick closure that can be attached without the use of tools. The reactor seal is established using a conical flange lock and O-ring seal of PTFE, FKM, or FFKM. The appropriate fitting inserts are available in stainless steel 1.4571 (SUS 316LTI) or Hastelloy C-22. A total of 6 connection options are provided in the lid, which can be selected from the following:
* Immersion tube for temperature probe
* Rupture disc of metal for safe limitation of the maximum pressure
* Pressure display 1 vent valve
* Vent valve
* 2 freely configurable fittings, for example for a gas sampling
Temperature is regulated using a temperature probe which detects the inner temperature of the reactor in an immersion tube. A second temperature probe can optionally be used as an independent overheating safety.
Features
* 300, 350, 500, 600ml / 200 bar / 300℃ (PTFE-Lined 230° )
* Quick closure ring, to be operated manually without tools
* O-seal ring made of Viton®, PTFE or Kalrez®
* Either with PTFE-insert or completely made of SUS 316LTl or Hastelloy®
* Heating and stirring by laboratory hot-plate with integrated magnetic stirrer (only 300-350ml)
* Heating by elctrical or thermostated mantle
* Stiring by magnetic clutch and separate drive
* Optionally internal heating/cooling coil
* Optionally 2’nd thermocouple
Technical Specification
| BR-500 | |||
| Material | SUS316Ti or HC | SUS316Ti PTFE | |
| Temperature max. | 300℃ | 230℃ | |
| Pressure max. | 200 bar | ||
| Reactor Vessel | Volume | approx. 630 ml | |
| Inner Diameter | 68 mm | ||
| Inner Height | 175 mm | ||
| Weight | approx. 6 kg | ||
| TFMTM-PTFE Insert* (integrated) | Volume | – | approx. 500 ml |
| Inner Diameter | – | 62.5 mm | |
| Inner Height | – | 165 mm | |
| Armatures | Standard Armatures | Rupture Disc, Dip Tube, Valve, Tool | |
| Pressure Measurement | analog and/or digital | ||
| Ports (total) | 6 | ||
| Ports (free) | 2** | ||
| Type of connection | 8 mm Tube Connection | ||
| Heating Systems (optional) | Electrical Heating mantle | CHM-500 | |
| Julabo thermostat | CTM-500 | ||
| Heating Coil | √ | ||
| Stirring | Magnetic stirrer | BLH-800 / 801 | |
| Overhead stirrer with magnetic clutch | WB20C and RV 100-SS | ||
| Stand | Pneumatic bench-top stand (with overhead stirrer)
Stand for BR-500 lid (with magnetic stirrer) |
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* When using PTFE inserts the maximum allowable temperature is 230℃
* The number of free ports can be enlarged by the use of T-connections
