This low-pressure reactor is ideally suitable for larger experimental runs. This low-pressure reactor is available in stainless steel, Hastelloy, or with PTFE lining on all sides. The usable volume of the reactor can be varied between 500ml, 1,000ml and 2,000 ml using different reactor vessels.
The NR-500/1000/2000 low-pressure reactor is notable for its ease of handling. The reactor is closed using a manual quick closure that can be attached without the use of tools. The reactor seal is established using a conical flange lock and O-ring seal of PTFE, FKM, or FFKM. The appropriate fitting inserts are available in stainless steel or Hastelloy. A total of 7 connection options are provided in the lid, which can be selected from the following:
* Gas sampling
* Rupture disc of metal for the safe limitation of maximum pressure
* Pressure display
* Vent valve
* Dip-tube liquid sampling
* Thermocouple with dip-tube
* Exhaust hose
Temperature is regulated using a temperature probe which detects the inner temperature of the reactor in an immersion tube. A second temperature probe can optionally be used as an independent overheating safety. Appropriate stand systems are available.
Features
* 500,1000 or 2000 ml / 25 bar / 300℃ (PTFE-Lined 230° )
* With or without bottom drain valve
* Quick closure chain, to be operated manually without tools
* O-seal ring made of Viton®, PTFE or Kalrez®
* Either with PTFE-insert or completely made of SUS 316L or Hastelloy®
* Heating by elctrical or thermostated mantle
* Stiring by magnetic clutch and separate drive
* Optionally internal heating/cooling coil
Technical Specification
| NR-100 | ||
| Material | Stainless Steel or Hastelloy | |
| Temperature max. | 300℃ | |
| Pressure max. | 25 bar | |
| Reactor Vessel | Volume | approx. 1000 ml |
| Inner Diameter | 96 mm | |
| Inner Height | 120 mm | |
| Weight | approx 5.7 kg | |
| Bottom Drain Valve | √ | |
| TFMTM-PTFE Insert | optional | |
| Armatures | Standard Armatures | Rupture Disc, Dip Tube, Valve, Tool |
| Pressure Measurement | analog and/or digital | |
| Ports (total) | 7 | |
| Ports (free) | 3 | |
| Type of connection | 8 mm Tube Connection | |
| Heating Systems | Via Fluid | with jacket |
| Via Fluid (Heating Coil, optional) | Heating coil | |
| Stirring | WB20C and RV 100-SS | |
| Stand | Pneumatic bench-top stand (M1 and M2)
Electric lifting stand (M3) |
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